3-乙酰基-2-甲基吡啶合成路线 （共 13 条）
反应条件
ammonium acetate in toluene Michael condensation; 24 h; Molecular sieveReflux; regioselective reaction;
参考文献
Allais, Christophe; Lieby-Muller, Frederic; Rodriguez, Jean; Constantieux, Thierry
European Journal of Organic Chemistry, 2013 , # 19 p. 4131 - 4145
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in water; N,N-dimethyl-formamide T=110°C; 1 h; Microwave irradiation; 2: With hydrogenchloride; water in methanol T=20°C;
参考文献
SANOFI; EL-AHMAD, Youssef; FILOCHE-ROMME, Bruno; GANZHORM, Axel; MARCINIAK, Gilbert; MUZET, Nicolas; RONAN, Baptiste; VIVET, Bertrand; ZERR, Véronique
Patent: WO2013/190123 A1, 2013 ;
Location in patent: Page/Page column 62 ;
反应条件
Keggin-type heteropolyacid T=20°C; 6 h; Neat (no solvent);
参考文献
Hekmatshoar, Rahim; Sadjadi, Sodeh; Sadjadi, Samaheh; Heravi, Majid M.; Beheshtiha, Yahya S.; Bamoharram, Fatemeh F.
Synthetic Communications, 2010 , vol. 40, # 11 p. 1708 - 1716
反应条件
in tetrahydrofuran T=-78 - 20°C;
参考文献
Chen, Liuhong; Cressina, Elena; Dixon, Neil; Erixon, Karl; Agyei-Owusu, Kwasi; Micklefield, Jason; Smith, Alison G.; Abell, Chris; Leeper, Finian J.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5924 - 5931
反应条件
diethyl ether; benzene Behandeln des Reaktionsgemisches mit wss.Schwefelsaeure;
参考文献
Journal of the American Chemical Society, , vol. 61, p. 2562
Takamine Kenkyusho Nenpo, , vol. 10, p. 27
Chem.Abstr., , p. 2634
反应条件
1: ethanol 2: 120 °C View Scheme
参考文献
Chemische Berichte, , vol. 90, p. 2265,2270
参考文献
Chemische Berichte, , vol. 72, p. 563,566
Chemische Berichte, , vol. 82, p. 117,119
参考文献
Chemische Berichte, , vol. 90, p. 2265,2270
参考文献
Chemische Berichte, , vol. 72, p. 563,566
Chemische Berichte, , vol. 82, p. 117,119
反应条件
1: sulfur; dioxane; aqueous <NH4>2S / 175 - 180 °C 2: P2O5 View Scheme
参考文献
Dornow; Schacht
Chemische Berichte, 1949 , vol. 82, p. 117,119
