反应条件
1: 1,6-dibromocyclohex-1-ene With trichlorosilane; triethylamine; copper(l) chloride in diethyl ether
T=15 - 23°C; Inert atmosphere;
2: methylmagnesium bromide in diethyl ether
T=0 - 23°C; Inert atmosphere;
3: With ammonium chloride in diethyl ether
T=0°C; Inert atmosphere;
参考文献
De Simone, Filippo; Andres, Julien; Torosantucci, Riccardo; Waser, Jerome
Organic Letters, 2009 , vol. 11, # 4 p. 1023 - 1026