1,6-二苯基-1,3,5-己三烯合成路线 (共 47 条)
反应条件
iron(II) oxalate dihydrate in N,N-dimethyl-formamide T=155 - 160°C; 0.75 h;
参考文献
Khurana, Jitender M.; Maikap, Golak C.; Mehta, Sanjay
Synthesis, 1990 , # 8 p. 731 - 732
反应条件
n-ethyl morpholine; palladium diacetate in xylene T=120°C; 8 h;
参考文献
Kasahara, Akira; Izumi, Taeko; Kudou, Naoto
Synthesis, 1988 , # 9 p. 704 - 705
反应条件
NbCl3 in tetrahydrofuran -10 deg C, 30 min, to rise to 20 deg C, 1,5 h and 5 h, 20 deg C;
参考文献
Szymoniak, Jan; Besancon, Jack; Moise, Claude
Tetrahedron, 1994 , vol. 50, # 9 p. 2841 - 2848
反应条件
triethylamine; palladium diacetate; tris-(o-tolyl)phosphine T=75 - 125°C; 6 h;
参考文献
Mitsudo, Taki-aki; Fischetti, William; Heck, Richard F.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1640 - 1646
反应条件
n-ethyl morpholine; palladium diacetate in xylene T=120°C; 8 h;
参考文献
Synthesis, , # 9 p. 704 - 705
反应条件
in dimethyl sulfoxide T=160°C; 5 h;
参考文献
Patro, Balaram; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Tetrahedron Letters, 1992 , vol. 33, # 6 p. 809 - 812
反应条件
palladium diacetate; triethylamine T=105°C; 24 h; Inert atmosphere;
参考文献
Mesganaw, Tehetena; Im, G-Yoon J.; Garg, Neil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3391 - 3393
反应条件
palladium diacetate; triethylamine T=105°C; 24 h; Inert atmosphere;
参考文献
Mesganaw, Tehetena; Im, G-Yoon J.; Garg, Neil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3391 - 3393
反应条件
dibromo-difluoro-methane; potassium hydroxide in dichloromethane T=0°C; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 1297 - 1300
反应条件
palladium diacetate; triethylamine T=105°C; 60 h; Inert atmosphere; Reagent/catalystSolventTemperature;
参考文献
Mesganaw, Tehetena; Im, G-Yoon J.; Garg, Neil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3391 - 3393