对甲苯磺酸2-甲氧基乙酯合成路线 （共 28 条）
反应条件
in pyridine T=0°C; 3.5 h;
参考文献
Heathcote, Robert; Howell, James A. S.; Jennings, Nicola; Cartlidge, David; Cobden, Lisa; Coles, Simon; Hursthouse, Michael
Dalton Transactions, 2007 , # 13 p. 1309 - 1315
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
TAIVEX THERAPEUTICS CORPORATION; HUANG, Yu-Ling; CHUANG, Shih-Hsien; LEE, Ying-Shuan Eda; HUANG, Jiann-Jyh; LAU, Johnson
Patent: WO2013/82324 A1, 2013 ;
Location in patent: Paragraph 00130 ;
反应条件
hydrogenchloride in pyridine; 2-methoxy-ethanol
反应条件
tetraethylammonium bromide T=165°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 710, p. 59 - 70
反应条件
sodium hydride 1.) THF, reflux, overnight, 2.) THF, reflux, 24 h; Yield given. Multistep reaction;
参考文献
Acta Chemica Scandinavica, , vol. 46, # 3 p. 278 - 282
反应条件
in ethanol T=74°C; 23 h;
参考文献
Heathcote, Robert; Howell, James A. S.; Jennings, Nicola; Cartlidge, David; Cobden, Lisa; Coles, Simon; Hursthouse, Michael
Dalton Transactions, 2007 , # 13 p. 1309 - 1315
反应条件
sodium hydride in pyridine T=20°C; 2 h; Product distribution / selectivity;
参考文献
Nanno, Tetsuo; Deguchi, Masaki
Patent: US2008/306308 A1, 2008 ;
Location in patent: Page/Page column 7-8 ;
反应条件
1: dibenzopyrrole With n-butyllithium in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: p-toluenesulfonic-acid-(2-methoxyethyl)-ester in tetrahydrofuran 2 h; Inert atmosphereCooling with ice;
参考文献
Kubota, Korefumi; Hirata, Shuzo; Yahiro, Masayuki; Adachi, Chihaya; Shibano, Yuki; Hirata, Osamu
Chemistry Letters, 2012 , vol. 41, # 9 p. 934 - 936,3
反应条件
hydrazine hydrate in ethanol 2 h;
参考文献
Osei-Twum, Emmanuel Y.; McCallion, Doug; Nazran, Avtar S.; Panicucci, Rick; Risbood, Prabhakar A.; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 336 - 342
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 6 p. 511 - 512
