2,2-二氟-2-(氟磺酰)醋酸盐合成路线 （共 68 条）
参考文献
Chen, Zili; Xiong, Wennan; Jiang, Biao
Chemical Communications, 2002 , # 18 p. 2098 - 2099
反应条件
1: T=0 - 100.6°C; P=4350.44 - 5925.59 Torr; 18 h; 2: With chloro-trimethyl-silane T=20 - 107.8°C; Heating / reflux; Product distribution / selectivity;
参考文献
Sievert, Allen Capron; Sprague, Lee G.
Patent: US2007/270602 A1, 2007 ;
Location in patent: Page/Page column 3-4 ;
反应条件
in neat (no solvent) at 5°C, with polytetrafluoroethylene filled reactor used; distn.;
参考文献
Dmitriev, M. A.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 966 - 969
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , p. 1035 - 1038
C.A., 1960 , p. 24341
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
water; Petroleum ether
反应条件
in petroleum ether with -10°C of H2O at 30-40°C;
参考文献
Journal of the American Chemical Society, , vol. 82, p. 6181 - 6188
F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
at 100°C, 2 h in autoclave;
参考文献
Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1243 - 1247
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1289 - 1294
C.A., 1968 , vol. 68, p. 12389
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
sodium sulfate in acetonitrile T=50°C; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 44, p. 433 - 440
反应条件
dehydrated H2SO4, 100°C, 20-25 torr;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
copper(l) iodide in acetonitrile T=50°C; 2 h;
参考文献
Chen, Qing-Yun; Wu, Sheng-Wen
Journal of Fluorine Chemistry, 1989 , vol. 44, p. 433 - 440
反应条件
sodium sulfate in acetonitrile T=45°C; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 44, p. 433 - 440
