2-(棕榈酰氧基)-1,3-丙烷二基(9E,9'E)二(-9-十八碳烯酸酯)合成路线 (共 12 条)
参考文献
Onodera, Junko; Matsuyama, Shigeru; Suzuki, Takahisa; Fujii, Koichi
Journal of chemical ecology, 2002 , vol. 28, # 6 p. 1209 - 1220
反应条件
lipozyme in hexane T=38°C;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 75, # 11 p. 1527 - 1531
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran T=55°C; 5 h;
参考文献
Chemistry and Physics of Lipids, , vol. 72, # 2 p. 185 - 191
反应条件
sodium methylate in hexane T=75°C; 0.5 h;
参考文献
Analytical Chemistry, , vol. 81, # 10 p. 3903 - 3910
反应条件
3 A molecular sieve; immobilized lipase from Rhizomucor miehei in hexane T=40°C;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 85, # 1 p. 47 - 53
反应条件
in toluene 4 h; Heating;
参考文献
Bhati, Asharam; Hamilton, Richard J.; Steven, David A.; Aneja, Rajender; Padley, Frederick B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 10 p. 1553 - 1558
反应条件
1: LiBr 2: hexamethylphosphoric triamide / tetrahydrofuran / 5 h / 55 °C View Scheme
参考文献
Chemistry and Physics of Lipids, , vol. 72, # 2 p. 185 - 191
反应条件
1: LiBr 2: hexamethylphosphoric triamide / tetrahydrofuran / 5 h / 55 °C View Scheme
参考文献
Chemistry and Physics of Lipids, , vol. 72, # 2 p. 185 - 191
反应条件
1: 95 percent Chromat. / EtOH, Rhizopus delemar lipase / various solvent(s) / 24 h / other lipases; var. solvents; var. carriers for lipase immobilization; also esterification with oleic acid 2: lipozyme / hexane / 38 °C View Scheme
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 75, # 11 p. 1527 - 1531
反应条件
1: 92 percent / pyridine / hexane / 30 min below 30 deg C then 4.5 h 2: 90 percent / toluene / 4 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 10 p. 1553 - 1558