二苯基(三甲基硅基)膦合成路线 （共 101 条）
参考文献
Dahl,O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1976 , vol. 30, p. 799 - 800
反应条件
cesium fluoride in N,N-dimethyl-formamide T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Reis, Andreas; Dehe, Daniel; Farsadpour, Saeid; Munstein, Isabel; Sun; Thiel, Werner R.
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2488 - 2495
反应条件
T=10°C; Addition; 0.5 h;
参考文献
Kabachnik; Khomutova; Beletskaya
Russian Chemical Bulletin, 1999 , vol. 48, # 12 p. 2352 - 2353
反应条件
1: 75 percent / diethyl ether / -80 deg C to -20 deg C 2: 80 °C View Scheme
参考文献
Lindner, Ekkehard; Steinwand, Michael; Hoehne, Sigurd
Chemische Berichte, 1982 , vol. 115, # 6 p. 2181 - 2191
反应条件
1: 82 percent / (MeCN)2PdCl2 / benzene / 100 h / 70 °C 2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C to RT View Scheme
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
反应条件
1: trimethyl-sulfonium iodide With n-butyllithium in tetrahydrofuran; hexane T=-70°C; 0.166667 h; 2: diphenyl(trimethylsilyl)phosphine in tetrahydrofuran; hexane T=-70 - 20°C; 0.5 h;
参考文献
Veits; Chuchuryukin; Neganova
Russian Journal of General Chemistry, 2002 , vol. 72, # 11 p. 1790 - 1792
反应条件
in acetonitrile 48 h; Ambient temperature;
参考文献
Russian Chemical Bulletin, , vol. 47, # 9 p. 1744 - 1748
反应条件
in benzene T=100°C; 2 h;
参考文献
Veits; Chuchuryukin; Neganova
Russian Journal of General Chemistry, 2002 , vol. 72, # 11 p. 1790 - 1792
反应条件
potassium alcoholate in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Uhlig, Frank; Hummeltenberg, Reinhard
Journal of Organometallic Chemistry, 1993 , vol. 452, # 1.2 p. C9 - C10
反应条件
dichloro bis(acetonitrile) palladium(II) in benzene T=70°C; 100 h;
参考文献
Tunney, S. E.; Stille, J. K.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 748 - 753
