1-氯-3-硝基-丙-2-醇合成路线 (共 6 条)
参考文献
Zhurnal Organicheskoi Khimii, , vol. 1, # 4 p. 636 - 640,636 - 639
反应条件
Lanthanum chloride; tetrabutylammomium bromide; sodium nitrite in diethyl ether; water
T=20°C; 6 h;
参考文献
Borah, Jagat C.; Gogoi, Siddhartha; Boruwa, Joshodeep; Barua, Nabin C.
Synthetic Communications, 2005 , vol. 35, # 6 p. 873 - 878
反应条件
potassium carbonate
T=45 - 50°C;
参考文献
I.G.Farbenind.
Patent: FR804589 ;
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I.G.Farbenind.
Patent: US2123556 , 1936 ;
反应条件
dinitrogen tetraoxide in diethyl ether
T=-15°C;
参考文献
Baskov,Yu.V.; Perekalin,V.V.
Doklady Chemistry, 1961 , vol. 136, p. 169 - 172
Doklady Akademii Nauk SSSR, 1961 , vol. 136, p. 1075 - 1078
反应条件
hydrogenchloride in diethyl ether
参考文献
Sokovishina,I.F. et al.
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, # 4 p. 636 - 640,636 - 639
反应条件
sulfuric acid in methanol
参考文献
Stotskii,A.A.; Okulovskaya,N.V.
Journal of Organic Chemistry USSR (English Translation), 1972 , vol. 8, # 11 p. 2305 - 2309
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, # 11 p. 2258 - 2263