5-甲基-1,5-己二烯-3-醇合成路线 （共 10 条）
参考文献
Wilson, R. Marshall; Rekers, John W.; Packard, Alan B.; Elder, R. C.
Journal of the American Chemical Society, 1980 , vol. 102, # 5 p. 1633 - 1641
反应条件
iodine; magnesium; ethylene dibromide in tetrahydrofuran T=20°C; ring opening; elimination; 8 h;
参考文献
Servi; Cansiz; Digrak; Ahmedzade
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 8 p. 629 - 633
参考文献
Akhmedov, M. A.; Vladimirova, I. I.; Kostikov, R. R.; Kyazimov, Sh. K.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 986 - 987
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 1097 - 1099
反应条件
(i) Mg, (ii) /BRN= 741856/; Multistep reaction;
参考文献
Dauben, William G.; Cogen, Jeffrey M.; Ganzer, George A.; Behar, Victor
Journal of the American Chemical Society, 1991 , vol. 113, # 15 p. 5817 - 5824
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 2.3.1.7, page 305 - 310
反应条件
(i) Ni(CO)4, benzene, (ii) /BRN= 741856/, DMF; Multistep reaction;
参考文献
Corey,E.J.; Semmelhack,M.F.
Journal of the American Chemical Society, 1967 , vol. 89, p. 2755 - 2757
参考文献
Bluthe, Norbert; Malacria, Max; Gore, Jacques
Tetrahedron, 1984 , vol. 40, # 17 p. 3277 - 3284
反应条件
chromium(VI) oxide; sulfuric acid in diethyl ether; water
T=0 - 20°C;
参考文献
Dauben, William G.; Cogen, Jeffrey M.; Ganzer, George A.; Behar, Victor
Journal of the American Chemical Society, 1991 , vol. 113, # 15 p. 5817 - 5824
反应条件
sodium acetate; pyridinium chlorochromate in dichloromethane
2 h; Product distribution; Further Variations:Reaction partnersReagentsSolvents;
参考文献
Servi; Cansiz; Acar; Koparir
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 11 p. 1542 - 1548
反应条件
1: PBr3 / diethyl ether / 15 h
2: (i) PhCH2NMe2, benzene-1,4-diol, toluene, (ii) aq. NaOH
View Scheme
参考文献
Spangler,C.W.; Woods,G.F.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2245 - 2248
