N-(3,4-二甲基苯基)-2-(羟基亚氨基)乙酰胺合成路线 (共 7 条)
反应条件
hydrogenchloride; hydroxylamine; sodium sulfate in water 1 h; Heating / reflux;
参考文献
TEIJIN LIMITED
Patent: EP1502916 A1, 2005 ;
Location in patent: Page 457 ;
EP 1502916 A1
反应条件
hydrogenchloride; hydroxylamine; sodium sulfate
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
反应条件
hydroxylamine hydrochloride; water; sodium sulfate
参考文献
King; Wright
Pr. roy. Soc. <B>, 1948 , vol. 135, p. 271,277
反应条件
1: With sulfuric acid in water T=85°C; 2 h; 2: With sodium hydroxide in water 3: With acetic acid in water pH=3;
参考文献
EP1505067 A1, ;
Page/Page column 375 ;
EP 1505067 A1
参考文献
Journal of Organic Chemistry, , vol. 17, p. 149,153
Proceedings of the Royal Society of London, Series B: Biological Sciences, , vol. 135, p. 271,291
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
Show Details
King; Wright
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1948 , vol. 135, p. 271,291
反应条件
1: sulfuric acid
3: aqueous NaOH
4: POCl3
5: palladium/charcoal; sodium acetate; acetic acid / 70 °C / Hydrogenation
View Scheme
参考文献
King; Wright
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1948 , vol. 135, p. 271,291