2-羟基亚氨基-N-(4-硝基苯基)-乙酰胺合成路线 (共 7 条)
反应条件
hydrogenchloride; hydroxylamine
参考文献
Garg, Rekha; Saini, Mahesh Kumar; Fahmi, Nighat; Singh
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2005 , vol. 44, # 12 p. 2433 - 2438
反应条件
hydroxylamine hydrochloride; sodium sulfate in water Condensation; substitution; 0.05 h; microwave irradiation;
参考文献
Jnaneshwara; Bedekar; Deshpande
Synthetic Communications, 1999 , vol. 29, # 20 p. 3627 - 3633
反应条件
1: conc. H2SO4 / Heating 2: 66 percent / Et3N / dimethylformamide / 1 h / 0 °C View Scheme
参考文献
Yamagishi; Yamada; Ozaki; Asao; Shimizu; Suzuki; Matsumoto; Matsuoka
Journal of Medicinal Chemistry, 1992 , vol. 35, # 11 p. 2085 - 2094
反应条件
1.1: sulfuric acid / 1.33 h / 50 - 65 °C 2.1: hydroxylamine hydrochloride / water / 0.5 h / |Reflux 2.2: 0.5 h 3.1: trichlorophosphate / 0 - 70 °C View Scheme
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
1.1: sulfuric acid / 1.33 h / 50 - 65 °C 2.1: hydroxylamine hydrochloride / water / 0.5 h / |Reflux 2.2: 0.5 h 3.1: trichlorophosphate / 0 - 70 °C 4.1: acetic acid / 3 h / |Reflux View Scheme
参考文献
Wang, Zheng; Wang, Cuiling; Sun, Yanni; Zhang, Ning; Liu, Zhulan; Liu, Jianli
Tetrahedron, 2014 , vol. 70, # 4 p. 906 - 913
反应条件
sulfuric acid Heating;
参考文献
Oezil, Musa; Mentese, Emre; Yilmaz, Fatih; Islamoglu, Fatih; Kahveci, Bahittin
Journal of Chemical Research, 2011 , vol. 35, # 5 p. 268 - 271
参考文献
Borsche; Fritzsche
Chemische Berichte, 1926 , vol. 59, p. 274