1,3,5-三甲基-2,4,6-三(3,5-二叔丁基-4-羟基苄基)苯合成路线 (共 8 条)
反应条件
sulfuric acid in acetic acid T=20 - 60°C; 6 h; Inert atmosphere;
参考文献
ALBEMARLE CORPORATION; SABAHI, Mahmood; NICHOLAS, Thomas, Robert
Patent: WO2011/5735 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
sulfuric acid in acetic acid T=60°C; 6 h;
参考文献
WO2011/5735 A1, ;
Page/Page column 9 ;
反应条件
sulfuric acid in acetic acid T=60°C; 3 h;
参考文献
WO2011/5735 A1, ;
Page/Page column 9 ;
反应条件
sulfuric acid in acetic acid T=20 - 60°C; 27 h; Inert atmosphere;
参考文献
WO2011/5735 A1, ;
Page/Page column 9-10 ;
反应条件
1: diethylamine / 11 h / Reflux 2: sulfuric acid / acetic acid / 6 h / 60 °C View Scheme
反应条件
1: diethylamine / 11 h / Reflux 2: sulfuric acid / acetic acid / 3 h / 60 °C View Scheme
反应条件
1: diethylamine / 11 h / Reflux 2: sulfuric acid / acetic acid / 27 h / 20 - 60 °C / Inert atmosphere View Scheme
反应条件
rate constant of the disproportionation; Rate constantThermodynamic data;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 34, p. 1833 - 1841
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 1987 - 1996