4-氨基-N,N-二甲基苯磺酰胺合成路线 （共 22 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol T=20°C; P=760.051 Torr; 6 h;
参考文献
WO2004/29066 A2, ;
Page/Page column 312-313 ;
反应条件
hydrogen; palladium on carbon in methanol
参考文献
WO2011/19405 A1, ;
Page/Page column 101-102 ;
WO 2011/019405 A1
反应条件
water; potassium hydroxide in methanol T=65°C; 24 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 71, p. 1 - 14
参考文献
WO2013/66640 A1, ;
Page/Page column 17 ;
反应条件
hydrogenchloride in ethanol; ethyl acetate; acetonitrile
反应条件
sodium hydroxide in methanol
反应条件
1: diethyl ether; H2O / 16 h / Ambient temperature 2: H2 / Raney-Ni / methanol / 20 h / 25 °C / 258.6 Torr View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 11 p. 1619 - 1633
反应条件
ammonium hydroxide T=250°C; P=139746 Torr;
参考文献
Journal of Organic Chemistry, , vol. 20, p. 1657,1661
反应条件
aluminum oxide; potassium hydroxide T=130°C; 0.0666667 h; microwave irradiation;
参考文献
Synthetic Communications, , vol. 38, # 18 p. 3074 - 3081
反应条件
1: benzene 2: aqueous hydrochloric acid View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 15, p. 525,528
