4-氨基-N,N-二乙基苯磺酰胺合成路线 （共 9 条）
反应条件
5 Pd(II)/C(eggshell); hydrogen in methanol 3 h;
参考文献
Gray, Vincent James; Wilden, Jonathan D.
Tetrahedron Letters, 2012 , vol. 53, # 1 p. 41 - 44
反应条件
1: With pyridine T=0 - 110°C; 4.16 h; 2: With hydrogenchloride; water in ethanol T=100°C; 3 h; 3: With sodium hydroxide in ethanol; water T=20°C; pH=~ 10;
参考文献
BIOLIPOX AB
Patent: WO2007/51982 A1, 2007 ;
Location in patent: Page/Page column 40 ;
反应条件
hydrogenchloride; trichlorophosphate in diethyl ether
反应条件
sodium hydroxide in water Deacetylation; 5 h; Heating;
参考文献
Kornev; Zheltov
Russian Journal of General Chemistry, 1999 , vol. 69, # 6 p. 962 - 968
反应条件
1: diethyl ether 2: aqueous hydrochloric acid View Scheme
参考文献
Biochemical Journal, , vol. 31, p. 724,727
反应条件
hydrogenchloride 1) Et2O, reflux; 2) reflux; Yield given. Multistep reaction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 7 p. 775 - 778
反应条件
1: 60 percent / H2O / 40 h / Heating
2: 73 percent / 50percent HCl, NaNO2 / H2O
3: acetic anhydride / 3 h / Heating
4: 38 percent / conc. HCl / ethanol; H2O / 2 h / Heating
View Scheme
参考文献
Tikare, Ravindra K.; Badami, Bharati V.; Puranik, Gurubasav S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 673 - 677
反应条件
in water
40 h; Heating;
参考文献
Tikare, Ravindra K.; Badami, Bharati V.; Puranik, Gurubasav S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 673 - 677
反应条件
1: 60 percent / H2O / 40 h / Heating
2: 73 percent / 50percent HCl, NaNO2 / H2O
View Scheme
参考文献
Tikare, Ravindra K.; Badami, Bharati V.; Puranik, Gurubasav S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 673 - 677
