反应条件
1: 1.) n-BuLi; 2.) ZnCl2 / 3.) Pd(PPh3)2Cl2 / 1.) THF, hexane, -78 deg C, 1 h; 2.) THF, hexane, RT, 1 h; 3.) THF, hexane, RT, 12 h 2: HCl / acetone / Ambient temperature View Scheme
参考文献
Balachari, Devan; Quinn, Liam; O'Doherty, George A.
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4769 - 4773