2-苯基-1,3-二氧六环-5-醇合成路线 (共 45 条)
反应条件
camphor-10-sulfonic acid in N,N-dimethyl-formamide T=70°C; 1 h;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
sodium hydroxide; sodium chloride; benzaldehyde in di-isopropyl ether; glycerol; toluene
反应条件
sulfuric acid T=40 - 45°C; P=10 Torr; 4 h; before heating 4 h room temperature; Yields of byproduct given;
参考文献
Carlsen, Per H. J.; Sorbye, Karsten; Ulven, Trond; Aasbo, Kari
Acta Chemica Scandinavica, 1996 , vol. 50, # 2 p. 185 - 187
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Chemistry Letters, , p. 1593 - 1596
反应条件
Candida cylindracea lipase Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 26 p. 2989 - 2992
反应条件
Candida cylindracea lipase Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 28, # 26 p. 2989 - 2992
反应条件
C40H50IrNP2 T=100°C; 1 h; Inert atmosphere; chemoselective reaction;
参考文献
Green Chemistry, , vol. 12, # 7 p. 1295 - 1300
反应条件
4 product ratio: trans/cis = 94/6; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 109, # 3 p. 908 - 910
反应条件
T=165°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 6613,6616
反应条件
1,1,3,3-tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate) in dichloromethane T=20°C;
参考文献
Zhang, Yin-Jie; Dayoub, Wissam; Chen, Guo-Rong; Lemaire, Marc
Green Chemistry, 2011 , vol. 13, # 10 p. 2737 - 2742