1-(4-氯苯基)-3-苯基-丙烷-1,3-二酮合成路线 （共 24 条）
反应条件
1: 35 percent / NCS / CCl4 / 12 h / Heating 2: dimethylsulfoxide / 3 h / 20 °C View Scheme
参考文献
Roshchupkina, Galina I.; Gatilov, Yury V.; Rybalova, Tatyana V.; Reznikov, Vladimir A.
European Journal of Organic Chemistry, 2004 , # 8 p. 1765 - 1773
反应条件
anhydrous iron chloride; tert.-butylnitrite T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Huang, Lehao; Cheng, Kai; Yao, Bangben; Xie, Yongju; Zhang, Yuhong
Journal of Organic Chemistry, 2011 , vol. 76, # 14 p. 5732 - 5737
反应条件
1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=20°C; 0.3 h; Inert atmosphere;
参考文献
Singh, Santosh; Singh, Pankaj; Rai, Vijai K.; Kapoor, Ritu; Yadav, Lal Dhar S.
Tetrahedron Letters, 2011 , vol. 52, # 1 p. 125 - 128
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=50°C; 1 h;
参考文献
Nandurkar, Nitin S.; Bhanushali, Mayur J.; Patil, Dinkar S.; Bhanage, Bhalchandra M.
Synthetic Communications, 2007 , vol. 37, # 23 p. 4111 - 4115
反应条件
lithium perchlorate; triethylamine in acetonitrile
20 h; Irradiation;
参考文献
Hasegawa, Eietsu; Ishiyama, Kenyuki; Horaguchi, Takaaki; Shimizu, Takahachi
Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1631 - 1635
反应条件
sodium hydride in tetrahydrofuran
0.5 h; Heating;
参考文献
Hasegawa, Eietsu; Ishiyama, Kenyuki; Horaguchi, Takaaki; Shimizu, Takahachi
Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1631 - 1635
反应条件
1: 89 percent / 31percent H2O2, 2N NaOH / methanol
2: 68 percent / NEt3, LiClO4 / acetonitrile / 20 h / Irradiation
View Scheme
参考文献
Hasegawa, Eietsu; Ishiyama, Kenyuki; Horaguchi, Takaaki; Shimizu, Takahachi
Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1631 - 1635
参考文献
Al-Hajjar, F.; Al-Sultan, Y.; Abushihada, A.; Shunbo, F.
Journal of Chemical & Engineering Data, 1980 , vol. 25, # 1 p. 83 - 85
反应条件
sodium hydroxide in dimethyl sulfoxide
参考文献
Wallet, Jean-Claude; Gaydou, Emile M.
Synthetic Communications, 1996 , vol. 26, # 22 p. 4097 - 4103
反应条件
hydrogenchloride; bromine; sodium methylate
1.) CHCl3, ice water bath, then 30 min, room t., 2.) MeOH, reflux, 1 h, 3.) MeOH, reflux, 15 min; Multistep reaction;
参考文献
Davis, Brian R.; Hinds, Mark G.
Australian Journal of Chemistry, 1997 , vol. 50, # 4 p. 309 - 319
