10-重氮基-9(10H)-蒽酮合成路线 （共 27 条）
反应条件
1: in tetrahydrofuran Barton-Kellogg reaction; 15 h; Inert atmosphere; 2: With triphenylphosphine in toluene Barton-Kellogg reaction; 24 h; Inert atmosphereReflux;
参考文献
Zhang, Xiaojie; Jiang, Xiaoxia; Zhang, Kai; Mao, Lu; Luo, Jing; Chi, Chunyan; Chan, Hardy Sze On; Wu, Jishan
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8069 - 8077
反应条件
fluorine in monofluoro-trichloromethane
参考文献
Patrick, Timothy B.; Scheibel, Jeffrey J.; Cantrell, Gary L.
Journal of Organic Chemistry, 1981 , vol. 46, # 19 p. 3917 - 3918
反应条件
Irradiation; Yield given. Yields of byproduct given;
参考文献
Field, Kurt W.; Schuster, Gary B.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4000 - 4006
参考文献
Cauquis,G.; Reverdy,G.
Bulletin de la Societe Chimique de France, 1975 , p. 1841 - 1844
反应条件
in tetrahydrofuran
2 h; Ambient temperatureother Grignard reagents; Mechanism;
参考文献
Bruni, Paolo; Carloni, Patricia; Conti, Carla; Giorgini, Elisabetta; Greci, Lucedio; Iacussi, Marco; Stipa, Pierluigi; Tosi, Giorgio
Tetrahedron, 1996 , vol. 52, # 19 p. 6795 - 6802
反应条件
1: 78 percent / benzene / 0.25 h / Irradiation
2: 2.) silver oxide / 1.) xylene, reflux, 3 h, 2.) benzene, 16 h
View Scheme
参考文献
Becker, Hans-Dieter; Elebring, Thomas
Journal of Organic Chemistry, 1985 , vol. 50, # 8 p. 1319 - 1322
反应条件
1: 13 percent / benzene / Irradiation
2: 12 percent / zinc / Ambient temperature
View Scheme
参考文献
Hirakawa, Kiyoichi; Nosaka, Toshikazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2835 - 2841
