10-重氮基-9(10H)-蒽酮合成路线 （共 27 条）
反应条件
4-dodecylbenzenesulphonyl azide; triethylamine in acetonitrile T=25°C;
参考文献
Hazen, George G.; Weinstock, Leonard M.; Connell, Robert; Bollinger, Frederick W.
Synthetic Communications, 1981 , vol. 11, # 12 p. 947 - 956
反应条件
piperidine; sodium azide; p-toluenesulfonyl chloride in ethanol; water T=20°C; 5 h;
参考文献
Levy, Amalia; Pogodin, Sergey; Cohen, Shmuel; Agranat, Israel
European Journal of Organic Chemistry, 2007 , # 31 p. 5198 - 5211
反应条件
15-crown-5; ADMC; triethylamine in tetrahydrofuran; acetonitrile T=-20°C; 0.166667 h;
参考文献
Kitamura, Mitsuru; Tashiro, Norifumi; Sakata, Rie; Okauchi, Tatsuo
Synlett, 2010 , # 16 p. 2503 - 2505
参考文献
Maas, Gerhard; Tretter, Andreas
Liebigs Annalen der Chemie, 1985 , # 9 p. 1866 - 1873
参考文献
Koerner, Michael; Rickborn, Bruce
Journal of Organic Chemistry, 1991 , vol. 56, # 4 p. 1373 - 1381
反应条件
1: acetonitrile 2: AcOH / aq. ethanol View Scheme
参考文献
Regitz,M.
Chemische Berichte, 1964 , vol. 97, p. 2742 - 2754
反应条件
in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Bruni, Paolo; Carloni, Patricia; Conti, Carla; Giorgini, Elisabetta; Greci, Lucedio; Iacussi, Marco; Stipa, Pierluigi; Tosi, Giorgio
Tetrahedron, 1996 , vol. 52, # 19 p. 6795 - 6802
反应条件
in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Bruni, Paolo; Carloni, Patricia; Conti, Carla; Giorgini, Elisabetta; Greci, Lucedio; Iacussi, Marco; Stipa, Pierluigi; Tosi, Giorgio
Tetrahedron, 1996 , vol. 52, # 19 p. 6795 - 6802
反应条件
in tetrahydrofuran 2 h; Ambient temperature; Further byproducts given;
参考文献
Bruni, Paolo; Carloni, Patricia; Conti, Carla; Giorgini, Elisabetta; Greci, Lucedio; Iacussi, Marco; Stipa, Pierluigi; Tosi, Giorgio
Tetrahedron, 1996 , vol. 52, # 19 p. 6795 - 6802
反应条件
in tetrahydrofuran 2 h; Ambient temperature; Further byproducts given;
参考文献
Bruni, Paolo; Carloni, Patricia; Conti, Carla; Giorgini, Elisabetta; Greci, Lucedio; Iacussi, Marco; Stipa, Pierluigi; Tosi, Giorgio
Tetrahedron, 1996 , vol. 52, # 19 p. 6795 - 6802
