1-对甲苯磺酰基-3-吡咯烷醇合成路线 （共 12 条）
反应条件
1: trimethyl-oxo-sulfonium iodide With n-butyllithium in tetrahydrofuran; hexane T=-78 - 0°C; 0.5 h; 2: 4-methyl-N-(oxiran-2-ylmethyl)benzenesulfonamide With N,N'-dimethyl-N,N'-propyleneurea in tetrahydrofuran; hexane 2 h; Heating; Further stages.;
参考文献
Chemical Communications, , # 30 p. 3226 - 3228
反应条件
boron trifluoride-tetrahydrofuran complex; iodosylbenzene in dichloromethane T=20°C; 4 h;
参考文献
Organic Letters, , vol. 16, # 5 p. 1442 - 1445
反应条件
tri-n-butyl-tin hydride in tetrahydrofuran 5 h; Heating;
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane Ambient temperature;
参考文献
Bioorganic & Medicinal Chemistry Letters, , vol. 9, # 10 p. 1379 - 1384
反应条件
iodosylbenzene; boron trifluoride diethyl etherate T=20°C; 0.25 h;
参考文献
Organic Letters, , vol. 16, # 5 p. 1442 - 1445
参考文献
US5281601 A1, ;
US 5281601 A
反应条件
1: 80.5 percent / NaH / dimethylformamide / 1 h / Ambient temperature 2: 75 percent / NBS, H2O / dimethylsulfoxide 3: 81 percent / (n-Bu)3SnH / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
1: 75 percent / NBS, H2O / dimethylsulfoxide 2: 81 percent / (n-Bu)3SnH / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 41, # 7 p. 1389 - 1398
反应条件
pyridinium chlorochromate in dichloromethane Ambient temperature;
参考文献
Kim, Wan-Joo; Kim, Bong-Jin; Lee, Tae-Suk; Nam, Keun-Soo; Kim, Keun-Jae
Heterocycles, 1995 , vol. 41, # 7 p. 1389 - 1398
