4-溴-5H-二苯并[a,d]环庚烯-5-酮合成路线 （共 6 条）
反应条件
sodium hydroxide in methanol T=20°C; Heating / reflux;
参考文献
Schering Corporation
Patent: US2004/122018 A1, 2004 ;
Location in patent: Page 213 ;
反应条件
sodium hydroxide in methanol 12 h; RefluxInert atmosphere;
参考文献
Kornmayer, Stefan C.; Rominger, Frank; Gleiter, Rolf
Synthesis, 2009 , # 15 art. no. T04509SS, p. 2547 - 2552
参考文献
Journal of the Chemical Society, Faraday Transactions, , vol. 90, # 21 p. 3273 - 3280
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in benzene 16 h; Irradiation;
参考文献
Mataka, Shuntaro; Liu, Guo-Bin; Tori-I, Akiyoshi; Tashiro, Masashi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 8 p. 2336 - 2338
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; sodium hydrogensulfite 1.) benzene, irrad., 22 h, 2.) benzene; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 8 p. 2336 - 2338
反应条件
(i) nBuLi, (ii) Br2, (iii) aq. HCl, THF; Multistep reaction;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 705, p. 169 - 184
