N,N-二甲基氨乙基乙二醇合成路线 (共 27 条)
反应条件
ammonia; Cr2Cu2O5 T=200°C; P=52505.3 Torr; Industry scale; Product distribution / selectivity;
参考文献
HUNTSMAN CORPORATION HUNGARY ZRt.; HUNTSMAN INTERNATIONAL LLC; GASPAR, Zsolt; HUMBERT, Heiko Heinrich; FELBER, Gabor; GASPAR, Attila; GRIGSBY, Robert Alison Jr.; KORDAS, Imre; VANDERSTRAETEN, Petra Emma
Patent: WO2010/139521 A1, 2010 ;
Location in patent: Page/Page column 17-23 ;
反应条件
hydrogen T=195°C; P=11879 Torr; 23.3 h; Compressed gas(es); Product distribution / selectivity;
参考文献
EP1505059 A1, ;
Page 5 ;
反应条件
hydrogen T=200°C; P=5931.67 Torr; Product distribution / selectivity;
参考文献
AIR PRODUCTS AND CHEMICALS, INC.
Patent: EP1505059 A1, 2005 ;
Location in patent: Page 6 ;
反应条件
ammonia; Cr2Cu2O5 T=200°C; P=52505.3 Torr; Industry scale; Product distribution / selectivity;
参考文献
HUNTSMAN CORPORATION HUNGARY ZRt.; HUNTSMAN INTERNATIONAL LLC; GASPAR, Zsolt; HUMBERT, Heiko Heinrich; FELBER, Gabor; GASPAR, Attila; GRIGSBY, Robert Alison Jr.; KORDAS, Imre; VANDERSTRAETEN, Petra Emma
Patent: WO2010/139521 A1, 2010 ;
Location in patent: Page/Page column 17-23 ;
参考文献
Nippon Shokubai Co., Ltd.
Patent: US5773669 A1, 1998 ;
反应条件
hydrogen T=195°C; P=11879 Torr; 23.3 h; Compressed gas(es); Product distribution / selectivity;
参考文献
EP1505059 A1, ;
Page 5 ;
反应条件
ammonia; Cr2Cu2O5 T=200°C; P=52505.3 Torr; Industry scale; Product distribution / selectivity;
参考文献
HUNTSMAN CORPORATION HUNGARY ZRt.; HUNTSMAN INTERNATIONAL LLC; GASPAR, Zsolt; HUMBERT, Heiko Heinrich; FELBER, Gabor; GASPAR, Attila; GRIGSBY, Robert Alison Jr.; KORDAS, Imre; VANDERSTRAETEN, Petra Emma
Patent: WO2010/139521 A1, 2010 ;
Location in patent: Page/Page column 17-23 ;
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran T=0 - 20°C; Mitsunobu reaction; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 53, # 15 p. 5844 - 5857
反应条件
ammonia; Cr2Cu2O5
T=200°C; P=52505.3 Torr; Industry scale; Product distribution / selectivity;
参考文献
HUNTSMAN CORPORATION HUNGARY ZRt.; HUNTSMAN INTERNATIONAL LLC; GASPAR, Zsolt; HUMBERT, Heiko Heinrich; FELBER, Gabor; GASPAR, Attila; GRIGSBY, Robert Alison Jr.; KORDAS, Imre; VANDERSTRAETEN, Petra Emma
Patent: WO2010/139521 A1, 2010 ;
Location in patent: Page/Page column 17-23 ;
反应条件
ammonia; 2CuO*Cr2O3
T=170°C; P=52505.3 Torr; Product distribution / selectivity;
参考文献
HUNTSMAN CORPORATION HUNGARY ZRT.; HUNTSMAN INTERNATIONAL LLC; HUMBERT, Heiko Heinrich; GASPAR, Zsolt; FELBER, Gabor; GASPAR, Attila; GRIGSBY, Robert Alison Jr.; KORDAS, Imre; VANDERSTRAETEN, Petra Emma
Patent: WO2010/139520 A1, 2010 ;
Location in patent: Page/Page column 24-28 ;