(2-氧代丙基)氨基甲酸叔丁酯合成路线 （共 8 条）
反应条件
in tetrahydrofuran T=-15 - 20°C;
参考文献
Liu, Jinchu; Ikemoto, Norihiro; Petrillo, Daniel; Armstrong III, Joseph D.
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8223 - 8226
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; Inert atmosphereCooling with ice;
参考文献
Mai, Duy N.; Rosen, Brandon R.; Wolfe, John P.
Organic Letters, 2011 , vol. 13, # 11 p. 2932 - 2935
反应条件
in tetrahydrofuran; diethyl ether 0.25 h;
参考文献
Nagafuji, Pamela; Cushman, Mark
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 4999 - 5003
反应条件
1: methanol / 1 h / 20 °C 2: 3.7 g / oxalyl chloride; DMSO; Et3N / CH2Cl2 / -55 - 0 °C View Scheme
参考文献
Synthesis, , # 6 p. 952 - 958
反应条件
tert.-butylhydroperoxide; silver hexafluoroantimonate; [Pd(Quinox)Cl2] in dichloromethane; water T=0 - 20°C; 2.5 h; Darkness;
参考文献
Michel, Brian W.; McCombs, Jessica R.; Winkler, Andrea; Sigman, Matthew S.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 40 p. 7312 - 7315
反应条件
hydrogenchloride in 1,4-dioxane 12 h;
参考文献
Chen, Li; Chen, Shaoqing; Michoud, Christophe
Patent: US2006/4046 A1, 2006 ;
Location in patent: Page/Page column 22 ;
US 20060004046 A1
参考文献
Wehrli
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 1915 - 1919
反应条件
formic acid; triethylamine; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; (1R,2R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine T=28°C; 24 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 16 p. 1916 - 1928
