2,2',4,4',5,5'-己甲氧基联苯合成路线 （共 41 条）
反应条件
[MoCl5] in dichloromethane
T=20°C; 0.5 h;
参考文献
Waldvogel, Siegfried R.
Synlett, 2002 , # 4 p. 622 - 624
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Yamaoka, Nobutaka; Sumida, Kohei; Itani, Itsuki; Kubo, Hiroko; Ohnishi, Yusuke; Sekiguchi, Sho; Dohi, Toshifumi; Kita, Yasuyuki
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 15004 - 15011
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Yamaoka, Nobutaka; Sumida, Kohei; Itani, Itsuki; Kubo, Hiroko; Ohnishi, Yusuke; Sekiguchi, Sho; Dohi, Toshifumi; Kita, Yasuyuki
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 15004 - 15011
反应条件
boron trifluoride diethyl etherate
参考文献
Douadi, Tahar; Cariou, Michel; Simonet, Jacques
Tetrahedron, 1996 , vol. 52, # 12 p. 4449 - 4456
反应条件
Et3NCH3 O3SOCH3; hexafluoroisopropyl alcohol
T=50°C; Electrolysis;
参考文献
Kirste, Axel; Schnakenburg, Gregor; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 5 p. 971 - 975
反应条件
trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=-78°C;
参考文献
Morimoto, Koji; Sakamoto, Kazuma; Ohnishi, Yusuke; Miyamoto, Takeshi; Ito, Motoki; Dohi, Toshifumi; Kita, Yasuyuki
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 8726 - 8731
反应条件
aluminium trichloride; nitrobenzene
参考文献
Baker; Evans
Journal of the Chemical Society, 1938 , p. 372,374
反应条件
1: sodium 2,4,5-trimethoxybenzoate With palladium (II) trifluoroacetate in dimethyl sulfoxide
T=80°C; 0.5 h; Inert atmosphere;
2: N-acetylindole With dimethyl sulfoxide; propionic acid in 1,4-dioxane
T=80°C; 15 h; Inert atmosphere;
参考文献
Zhou, Jun; Hu, Peng; Zhang, Min; Huang, Shijun; Wang, Min; Su, Weiping
Chemistry - A European Journal, 2010 , vol. 16, # 20 p. 5876 - 5881
反应条件
trimethylsilyl trifluoromethanesulfonate in hexafluoroisopropyl alcohol
T=20°C; 3 h; Inert atmosphere;
参考文献
Dohi, Toshifumi; Ito, Motoki; Yamaoka, Nobutaka; Morimoto, Koji; Fujioka, Hiromichi; Kita, Yasuyuki
Angewandte Chemie - International Edition, 2010 , vol. 49, # 19 p. 3334 - 3337
反应条件
Et3NCH3 O3SOCH3; hexafluoroisopropyl alcohol
T=50°C; Electrolysis;
参考文献
Kirste, Axel; Schnakenburg, Gregor; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 5 p. 971 - 975
