2,3,4,5-四氢-1H-苯并[b]氮杂卓合成路线 （共 35 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Robichaud, Albert J.; Lee, Taekyu; Deng, Wei; Mitchell, Ian S.; Chen, Wenting; McClung, Christopher D.; Calvello, Emilie J.; Zawrotny, David M.
Patent: US2004/209864 A1, 2004 ;
US 20040209864 A1
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 23 h; 2: With sodium hydroxide; water in tetrahydrofuran
参考文献
MADDAFORD, Shawn; RAMNAUTH, Jailall; RAKHIT, Suman; PATMAN, Joanne; ANNEDI, Subhash C.; ANDREWS, John; DOVE, Peter; SILVERMAN, Sarah; Renton, Paul
Patent: US2008/234237 A1, 2008 ;
Location in patent: Page/Page column 72 ;
US 20080234237 A1
反应条件
diisobutylaluminium hydride in dichloromethane T=0°C; 1 h;
参考文献
Sasatani, Satoru; Miyazaki, Tohru; Maruoka, Keiji; Yamamoto, Hisashi
Tetrahedron Letters, 1983 , vol. 24, # 43 p. 4711 - 4712
反应条件
bis(acetylacetonate)nickel(II); sodium t-butanolate; IPr*hydrochloride in 1,4-dioxane T=100°C; 11 h;
参考文献
Omar-Amrani, Rafik; Thomas, Antoine; Brenner, Eric; Schneider, Raphael; Fort, Yves
Organic Letters, 2003 , vol. 5, # 13 p. 2311 - 2314
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; potassium carbonate in toluene T=111°C; 20 h;
参考文献
Fujita, Ken-Ichi; Yamamoto, Kazunari; Yamaguchi, Ryohei
Organic Letters, 2002 , vol. 4, # 16 p. 2691 - 2694
反应条件
1: With diisobutylaluminium hydride in dichloromethane 2: With NAF in dichloromethane regioselective reaction;
参考文献
Iwama, Yusuke; Okano, Kentaro; Sugimoto, Kenji; Tokuyama, Hidetoshi
Chemistry - A European Journal, 2013 , vol. 19, # 28 p. 9325 - 9334
反应条件
C2Cl2O2Rh(1-)*C32H32N2O2Rh(1+); hydrogen in tetrahydrofuran T=100°C; P=5171.62 - 36201.3 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 51, # 38 p. 4959 - 4961
反应条件
potassium hydroxide; hydrazine in water; diethylene glycol 6 h; Heating / reflux;
参考文献
WO2006/122156 A2, ;
Page/Page column 125 ;
WO 2006/122156 A2
反应条件
C2Cl2O2Rh(1-)*C8H16N2O2Rh(1+); hydrogen in toluene T=100°C; P=5171.62 - 36201.3 Torr; 24 h;
参考文献
Tetrahedron Letters, , vol. 51, # 38 p. 4959 - 4961
反应条件
BH3 in tetrahydrofuran
参考文献
Pfizer Inc.
Patent: US5736534 A1, 1998 ;
