3,4-二苄氧基-反-β-硝基苯乙烯合成路线 (共 8 条)
反应条件
ammonium acetate; acetic acid Henry reaction; 0.666667 h; Heating;
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.; Cowley, Andrew
Tetrahedron, 2004 , vol. 60, # 16 p. 3695 - 3712
参考文献
Clairol Incorporated
Patent: US4595765 A1, 1986 ;
反应条件
1: 99 percent / K2CO3 / dimethylformamide / 15 h / 120 °C 2: 98 percent / ammonium acetate; acetic acid / 0.67 h / Heating View Scheme
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.; Cowley, Andrew
Tetrahedron, 2004 , vol. 60, # 16 p. 3695 - 3712
反应条件
1: 99 percent / K2CO3 / dimethylformamide / 15 h / 120 °C 2: 98 percent / ammonium acetate; acetic acid / 0.67 h / Heating View Scheme
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.; Cowley, Andrew
Tetrahedron, 2004 , vol. 60, # 16 p. 3695 - 3712
反应条件
1: 97 percent / acetic acid; HNO3 / H2O / 2 h / 20 °C 2: 61 percent / iron; acetic acid; SiO2 / benzene; cyclohexane / 0.5 h / Heating View Scheme
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.; Cowley, Andrew
Tetrahedron, 2004 , vol. 60, # 16 p. 3695 - 3712
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 1.25 h / Heating 2: sodium hydrogen carbonate / CH2Cl2; H2O / 1.5 h 3: phosphorus oxychloride / acetonitrile / 0.42 h / Heating 4: sodium borohydride / methanol / 0.75 h / 0 °C 5: hydrogen, conc. hydrochloric acid / 10percent palladium-charcoal / ethanol / 2 h View Scheme
参考文献
Battersby, Alan R.; Jones, Raymond C. F.; Kazlauskas, Rymantas; Thornber, Craig W.; Ruchirawat, Somsak; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2016 - 2029
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1.25 h; Heating;
参考文献
Battersby, Alan R.; Jones, Raymond C. F.; Kazlauskas, Rymantas; Thornber, Craig W.; Ruchirawat, Somsak; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2016 - 2029
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in ethanol P=760 Torr; 24 h; Ambient temperature;
参考文献
Kohno; Sasao; Murahashi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1252 - 1254