3,4-二氢异喹啉-2(1h)-甲醛合成路线 （共 30 条）
反应条件
sodium hydroxide in ethanol 4 h; Ambient temperature;
参考文献
Shinohara, Tatsumi; Toda, Jun; Sano, Takehiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 5 p. 813 - 819
反应条件
1: in chloroform
T=0 - 20°C; 1 h;
2: With hydrogenchloride in dichloromethane; chloroform; water
3: With sodium hydrogencarbonate in dichloromethane; chloroform; water
参考文献
MITSUBISHI PHARMA CORPORATION
Patent: WO2004/87124 A1, 2004 ;
Location in patent: Page/Page column 44 ;
WO 2004/087124 A1
反应条件
water; Rh6(CO)12 in 2-methoxy-ethanol
T=150°C; P=41188.4 Torr; 24 h;
参考文献
Murahashi; Imada; Hirai
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 2968 - 2976
反应条件
potassium hydroxide; carbon monoxide; water; pentacarbonyliron(0) in methanol
T=300°C; P=20685.9 - 51714.8 Torr; 1 h;
参考文献
Lynch, Thomas J.; Banah, Mahmoud; Kaesz, Herbert D.; Porter, Clifford R.
Journal of Organic Chemistry, 1984 , vol. 49, # 7 p. 1266 - 1270
反应条件
styrene; [Ru(η4-COD)(η3-methylallyl)2]; potassium tert-butylate; ICy*HCl in toluene
T=125°C; 24 h; Inert atmosphereGlovebox;
参考文献
Ortega, Nuria; Richter, Christian; Glorius, Frank
Organic Letters, 2013 , vol. 15, # 7 p. 1776 - 1779
反应条件
Rh6(CO)12; water in 2-methoxy-ethanol
T=150°C; P=41188.4 Torr; 24 h;
参考文献
Murahashi; Imada; Hirai
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 2968 - 2976
反应条件
palladium/alumina; hydrogen in octane
T=130°C; P=22502.3 Torr; 24 h; Autoclave;
参考文献
Cui, Xinjiang; Zhang, Yan; Deng, Youquan; Shi, Feng
Chemical Communications, 2014 , vol. 50, # 2 p. 189 - 191
反应条件
sodium hydroxide in ethanol; water
T=27°C; 9 h;
参考文献
Preedasuriyachai, Patcharee; Kitahara, Hiroaki; Chavasiri, Warinthorn; Sakurai, Hidehiro
Chemistry Letters, 2010 , vol. 39, # 11 p. 1174 - 1176
反应条件
tris(2,2,2-trifluoroethyl) borate in acetonitrile
T=100°C; 5 h; Sealed tube; Time;
参考文献
Lanigan, Rachel M.; Starkov, Pavel; Sheppard, Tom D.
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4512 - 4523
反应条件
palladium 10 on activated carbon
T=150°C; 3 h;
参考文献
Kulkarni, Aditya; Gianatassio, Ryan; Toeroek, Bela
Synthesis, 2011 , # 8 art. no. M09611SS, p. 1227 - 1232
