10-溴-7H-苯并[c]咔唑合成路线 （共 6 条）
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=0°C; 24 h;
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; LEE, Hyo-jung; KIM, Hye-mi; LEE, Soo-yong; PARK, Kyoung-jin; LEE, Su-hyun; AHN, Hee-choon; KIM, Nam-kyun; KU, Jong-seok; KWON, Hyuck-joo; LEE, Kyung-joo; KIM, Bong-ok
Patent: WO2013/32297 A1, 2013 ;
Location in patent: Paragraph 147; 148 ;
反应条件
sodium hydrogensulfite in water T=120°C; 12 h;
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD; LEE, Soo Young; CHO, Young Jun; KIM, Bong Ok; KIM, Sung Min
Patent: WO2012/15265 A1, 2012 ;
Location in patent: Page/Page column 14-15 ;
反应条件
hydrogenchloride; Na2S2O5 in water Heating;
参考文献
Hill; Eaddy
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 8 p. 697 - 706
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; ethanol / 3 h / 90 °C 2: triethyl phosphite / 24 h / 150 °C 3: N-bromosuccinmide / N,N-dimethyl-formamide / 24 h / 0 °C View Scheme
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; AHN, Hee-choon; YOON, Seok-keun; KIM, Nam-kyun; KIM, Seung-ae; KU, Jong-seok; KWON, Hyuck-joo; LEE, Kyung-joo; KIM, Bong-ok
Patent: WO2013/73874 A1, 2013 ;
反应条件
1: triethyl phosphite / 24 h / 150 °C 2: N-bromosuccinmide / N,N-dimethyl-formamide / 24 h / 0 °C View Scheme
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; AHN, Hee-choon; YOON, Seok-keun; KIM, Nam-kyun; KIM, Seung-ae; KU, Jong-seok; KWON, Hyuck-joo; LEE, Kyung-joo; KIM, Bong-ok
Patent: WO2013/73874 A1, 2013 ;
反应条件
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; ethanol / 3 h / 90 °C 2: triethyl phosphite / 24 h / 150 °C 3: N-bromosuccinmide / N,N-dimethyl-formamide / 24 h / 0 °C View Scheme
参考文献
ROHM AND HAAS ELECTRONIC MATERIALS KOREA LTD.; LEE, Hyo-jung; KIM, Hye-mi; LEE, Soo-yong; PARK, Kyoung-jin; LEE, Su-hyun; AHN, Hee-choon; KIM, Nam-kyun; KU, Jong-seok; KWON, Hyuck-joo; LEE, Kyung-joo; KIM, Bong-ok
Patent: WO2013/32297 A1, 2013 ;
