N,N-二乙基苯甲酰胺合成路线 (共 244 条)
反应条件
T=230°C; P=15001.5 Torr; 0.0833333 h; microwave irradiation;
参考文献
US2010/81843 A1, ;
Page/Page column 6 ;
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; 1 h; Inert atmosphereSchlenk technique; Overall yield = 49 percent;
参考文献
Tetrahedron, , vol. 69, # 46 p. 9580 - 9585
反应条件
iron (III) acetylacetonate in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; 1 h; Inert atmosphereSchlenk technique; Overall yield = 81 percent;
参考文献
Tetrahedron, , vol. 69, # 46 p. 9580 - 9585
反应条件
[Bmim][PdI2](PPh3); potassium carbonate in dichloromethane T=90°C; P=15001.5 Torr; 5 h; Autoclave;
参考文献
Applied Organometallic Chemistry, , vol. 28, # 1 p. 48 - 53
反应条件
PdCl2(PMePh2)2 in neat (no solvent) T=100°C; P=7600 Torr; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 107, # 11 p. 3235 - 3245
反应条件
1: With Ph2CuLi*LiCN in diethyl ether T=0°C; 0.5 h; 2: With water; ammonium chloride in diethyl ether
参考文献
Cetin, Fatma; Baris Senogul; Gezer, Sibel; Astley, Demet; Astley, Stephen T.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 1 p. 154 - 157
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran T=20°C; 2 h;
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
sodium hydroxide; potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate in benzene 3.5 h; Heating;
参考文献
Gajda, Tadeusz; Zwierzak, Andrzej
Synthesis, 1981 , # 12 p. 1005 - 1008
反应条件
1: anhydrous diethylamine hydrochloride With diisobutylaluminium hydride in tetrahydrofuran; toluene 2: benzoic acid ethyl ester in tetrahydrofuran T=45°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 42, # 51 p. 9039 - 9041
反应条件
bis(acetylacetonate)nickel(II); di-isopropylmagnesium in diethyl ether T=20°C;
参考文献
Milburn, Robert R.; Snieckus, Victor
Angewandte Chemie - International Edition, 2004 , vol. 43, # 7 p. 888 - 891