2,4,6-三甲基-1,3-次苯基二异氰酸盐合成路线 (共 3 条)
反应条件
tributylphosphine; di-isopropyl azodicarboxylate in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Saylik, Dilek; Horvath, Michael J.; Elmes, Patricia S.; Jackson, W. Roy; Lovel, Craig G.; Moody, Keith
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3940 - 3946
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 0.166667 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias; Schlechtingen, Georg
Angewandte Chemie, 1995 , vol. 107, # 22 p. 2746 - 2749
反应条件
palladium(IV) oxide; MoO3+Fe2O3 on Al2O3 in 1,2-dichloro-benzene T=210°C; P=228000 Torr;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 29, # 1 p. 117 - 120
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 133 - 136