溴化(3-丁烯-1-YL)三苯基磷合成路线 （共 4 条）
反应条件
in toluene 24 h; Inert atmosphereReflux;
参考文献
Yang, Qingliang; Draghici, Cristian; Njardarson, Jon T.; Li, Fang; Smith, Brandon R.; Das, Pradipta
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 330 - 344
参考文献
Drouin, J.; Leyendecker, F.; Conia, J. M.
Tetrahedron, 1980 , vol. 36, # 82 p. 1195 - 1202
反应条件
n-butyllithium in tetrahydrofuran; hexane
参考文献
Winter,M. et al.
Helvetica Chimica Acta, 1979 , vol. 62, p. 135 - 139
反应条件
1: but-3-enyltriphenylphosphonium bromide With potassium hexamethylsilazane in tetrahydrofuran
T=-78°C; 1 h; Inert atmosphere;
2: methyl chloroformate in tetrahydrofuran
T=-78 - 20°C; 1.5 h; Inert atmosphere;
参考文献
Yang, Qingliang; Draghici, Cristian; Njardarson, Jon T.; Li, Fang; Smith, Brandon R.; Das, Pradipta
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 330 - 344
