hydrogen; triethylamine; {RuHCl((R)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl)2} in tetrahydrofuran; ethanol T=50°C; P=2280 Torr; 24 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 428, # 1-2 p. 155 - 167
ammonium cerium (IV) nitrate in water; acetonitrile T=20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Garcia, Jesus M.; Gonzalez, Alberto; Kardak, Bharat G.; Odriozola, Jose M.; Oiarbide, Mikel; Razkin, Jesus; Palomo, Claudio
Chemistry - A European Journal, 2008 , vol. 14, # 29 p. 8768 - 8771
1: With (CuOTf)2.C6H6; (2-diphenylphosphinobenzoyl)-Thr(O-t-Bu)-D-Val-NH-n-butyl in toluene T=0°C; 1.3 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 11 p. 1276 - 1279