1-甲氧基-4-((E)-苯乙烯基)-苯合成路线 (共 30 条)
反应条件
diethyl ether T=180°C;
参考文献
Sanabo G.m.b.H.
Patent: DE701402 , 1938 ;
DRP/DRBP Org.Chem.
反应条件
9,10-anthracenedicarbonitrile in acetonitrile IrradiationΦsep, -ΔG-et; other electron acceptors; quantum yield for separation of initially formed radical ion pair to generate free stilbene cation radical; Quantum yieldThermodynamic data;
参考文献
Hara, Michihiro; Samori, Shingo; Xichen, Cai; Fujitsuka, Mamoru; Majima, Tetsuro
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4370 - 4374
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=40°C; Irradiation; Yield given;
参考文献
Woning, Jan; Oudenampsen, Albert; Laarhoven, Wim H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 2147 - 2154
反应条件
in acetonitrile UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4279 - 4282
反应条件
[bis(acetoxy)iodo]benzene; ammonium hydrogen carbonate in methanol; water T=36°C; 12 h; Sealed tube;
参考文献
Journal of Organic Chemistry, , vol. 78, # 23 p. 11881 - 11886
反应条件
potassium phosphate; Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide in water; N,N-dimethyl-formamide
T=85°C; Heck coupling; 6 h;
参考文献
Lee, Dong-Hwan; Taher, Abu; Hossain, Shahin; Jin, Myung-Jong
Organic Letters, 2011 , vol. 13, # 20 p. 5540 - 5543
反应条件
palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide
T=130°C; Heck reaction; 48 h; Inert atmosphere; optical yield given as percent deregioselective reaction;
参考文献
Limberger, Jones; Poersch, Silvia; Monteiro, Adriano L.
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 7 p. 1389 - 1394
反应条件
T=800°C; P=0.01 Torr;
参考文献
Chu, Li-Tse; Yu, Pin-Chih; Wu, Bo-Jian; Liao, Ying-Chi; Chou, Chin-Hsing
Heterocycles, 2007 , vol. 71, # 1 p. 165 - 173
反应条件
10 Pd on charcoal; diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in ethanol
4 h; Reflux;
参考文献
Liu, Qiang; Li, Jing; Shen, Xiao-Xia; Xing, Rui-Guang; Yang, Jie; Liu, Zhengang; Zhou, Bo
Tetrahedron Letters, 2009 , vol. 50, # 9 p. 1026 - 1028
反应条件
T=25°C; 0.0333333 h; UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1480 - 1492