(1R,2r,5r)-2-异丙基-5-甲基环己胺合成路线 （共 8 条）
反应条件
methanol; nickel T=106°C; P=73550.8 Torr; Hydrogenation;
参考文献
Journal of the Chemical Society, , p. 153,157
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 40 h; Inert atmosphereReflux;
参考文献
Canadian Journal of Chemistry, , vol. 89, # 10 p. 1222 - 1229
反应条件
1: (i) CrO3, H2SO4, (ii) NH2OH 2: Na / ethanol View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 707, p. 78 - 86
反应条件
1: pyridine; hydroxylamine hydrochloride / ethanol / 40 h / Inert atmosphere; Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 40 h / 0 °C / Inert atmosphere; Reflux View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 89, # 10 p. 1222 - 1229
反应条件
anschliessend Verseifen der entstandenen Formylderivate mit Salzsaeure; Trennung erfolgt durch Unsetzung mit Salicylaldehyd und Hydrolyse des ausgeschiedenen Salicylidenderivats mit verd. Schwefelsaeure;
参考文献
Journal of the Chemical Society, , p. 2173
反应条件
palladium on activated charcoal; 4 A molecular sieve; hydrogen; tin(IV) chloride; benzylamine other amines; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 15 p. 3102 - 3108
反应条件
Verseifen der entstandenen Formylderivate mit Salzsaeure;
参考文献
Journal of the Chemical Society, , p. 1278
Journal of the Chemical Society, , vol. 85, p. 74
Journal of the Chemical Society, , p. 2218
Journal of the Chemical Society, , p. 2171
Justus Liebigs Annalen der Chemie, , vol. 276, p. 306
Justus Liebigs Annalen der Chemie, , vol. 300, p. 278
反应条件
water; sodium nitrite
partial inactivated dextrorotatory menthenesubstances;
参考文献
Read; Robertson; Cook
Journal of the Chemical Society, 1927 , p. 1278
Full Text Show Details
Read; Robertson
Journal of the Chemical Society, 1926 , p. 2218
Journal of the Chemical Society, 1927 , p. 2171
