2-(Boc-氨基)-3-丁醇合成路线 （共 12 条）
反应条件
caesium carbonate in methanol
参考文献
Berkowitz, David B.; Bose, Mohua; Choi, Sungjo
Angewandte Chemie - International Edition, 2002 , vol. 41, # 9 p. 1603 - 1607
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene desulfurization; 1 h; Heating;
参考文献
Bach, Thorsten; Koerber, Christina
Journal of Organic Chemistry, 2000 , vol. 65, # 8 p. 2358 - 2367
反应条件
1: 78 percent / ceric ammonium nitrate / acetonitrile; H2O 2: 88 percent / triethylamine / CH2Cl2 3: 88 percent / Cs2CO3 / methanol View Scheme
参考文献
Berkowitz, David B.; Bose, Mohua; Choi, Sungjo
Angewandte Chemie - International Edition, 2002 , vol. 41, # 9 p. 1603 - 1607
反应条件
1: 88 percent / triethylamine / CH2Cl2 2: 88 percent / Cs2CO3 / methanol View Scheme
参考文献
Berkowitz, David B.; Bose, Mohua; Choi, Sungjo
Angewandte Chemie - International Edition, 2002 , vol. 41, # 9 p. 1603 - 1607
反应条件
1: 89 percent / LiHMDS; PPh3; [Ni(cod)2] / tetrahydrofuran; hexane / 1 h 2: 78 percent / ceric ammonium nitrate / acetonitrile; H2O 3: 88 percent / triethylamine / CH2Cl2 4: 88 percent / Cs2CO3 / methanol View Scheme
参考文献
Berkowitz, David B.; Bose, Mohua; Choi, Sungjo
Angewandte Chemie - International Edition, 2002 , vol. 41, # 9 p. 1603 - 1607
反应条件
sodium hydrogencarbonate in methanol; water; ethyl acetate Acylation; biphasic;
参考文献
Sabat, Mark; Johnson, Carl R.
Organic Letters, 2000 , vol. 2, # 8 p. 1089 - 1091
反应条件
1: 70 percent / FeCl2 / CH2Cl2 / 20 °C 2: 71 percent / Bu3SnH; AIBN / benzene / 1 h / Heating View Scheme
参考文献
Bach, Thorsten; Koerber, Christina
Journal of Organic Chemistry, 2000 , vol. 65, # 8 p. 2358 - 2367
反应条件
1: 48 percent / Pseudomonas cepecia (Amano PS-30) lipase / CH2Cl2 / 20 °C / Enzymatic reaction 2: 96 percent / KCN / methanol / 20 °C 3: BF3*Et2O / acetone / -20 - 20 °C View Scheme
参考文献
Sabat, Mark; Johnson, Carl R.
Organic Letters, 2000 , vol. 2, # 8 p. 1089 - 1091
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone
参考文献
Berkowitz, David B.; Bose, Mohua; Choi, Sungjo
Angewandte Chemie - International Edition, 2002 , vol. 41, # 9 p. 1603 - 1607
反应条件
1: 46 percent / Pseudomonas cepecia (Amano PS-30) lipase / CH2Cl2 / 20 °C / Enzymatic reaction
2: BF3*Et2O / acetone / -20 - 20 °C
View Scheme
参考文献
Sabat, Mark; Johnson, Carl R.
Organic Letters, 2000 , vol. 2, # 8 p. 1089 - 1091
