1-溴-2,6-二甲氧基苯合成路线 （共 37 条）
反应条件
perchloric acid; dihydrogen peroxide; potassium bromide; NH4VO3 in water; acetonitrile 24 h; Ambient temperature;
参考文献
Sauer, Marc; Yeung, Charles; Chong, Jonathan H.; Patrick, Brian O.; MacLachlan, Mark J.
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 775 - 788
反应条件
silver carbonate; copper(ll) bromide; palladium dichloride in tetrahydrofuran T=110°C; 24 h;
参考文献
Peng, Xuefeng; Shao, Xiang-Feng; Liu, Zhong-Quan
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3079 - 3081
反应条件
n-butyllithium in diethyl ether; hexane; water
参考文献
Sumitomo Chemical Co., Ltd.
Patent: US5621129 A1, 1997 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Weimar, Marko; Duerner, Gerd; Bats, Jan W.; Goebel, Michael W.
Journal of Organic Chemistry, 2010 , vol. 75, # 8 p. 2718 - 2721
反应条件
1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=0 - 25°C; 5 h; Inert atmosphere; 2: 4,5-dibromoveratrole in tetrahydrofuran; hexane T=-35 - 25°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 2 p. 341 - 354
反应条件
1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=0 - 25°C; 5 h; Inert atmosphere; 2: 4,5-dibromo-o-xylene in tetrahydrofuran; hexane T=-78 - 25°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 2 p. 341 - 354
反应条件
1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=0 - 25°C; 5 h; Inert atmosphere; 2: ortho-dibromobenzene in tetrahydrofuran; hexane T=0 - 25°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 2 p. 341 - 354
反应条件
1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=0 - 25°C; 5 h; Inert atmosphere; 2: 2,3-dibromo-1,4-dimethylbenzene in tetrahydrofuran; hexane T=0 - 25°C; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 2 p. 341 - 354
反应条件
N-bromosuccinmide in methanol 1 h; Ambient temperature;
参考文献
Wada, Masanori; Wakamori, Hiroyuki; Hiraiwa, Akira; Erabi, Tatsuo
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1389 - 1391
反应条件
copper(ll) bromide in methanol Heating;
参考文献
Thompson, Alicia L. S.; Kabalka, George W.; Akula, Murthy R.; Huffman, John W.
Synthesis, 2005 , # 4 art. no. M05304SS, p. 547 - 550
