2,6-二甲氧基-1-碘苯合成路线 （共 33 条）
反应条件
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; cobalt(II) dibromide in tetrahydrofuran; hexane T=0 - 20°C; 0.5 h; 2: With iodine in tetrahydrofuran; hexane T=20°C; 2 h; 3: With water; sodium thiosulfate in tetrahydrofuran; hexane regioselective reaction;
参考文献
Dayaker, Gandrath; Chevallier, Floris; Gros, Philippe C.; Mongin, Florence
Tetrahedron, 2010 , vol. 66, # 46 p. 8904 - 8910
反应条件
iodine; oxygen; H5PV2Mo10O40 in acetonitrile-D3 T=80°C; P=1520 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 24 p. 9510 - 9512
反应条件
N-iodo-succinimide in acetonitrile T=25°C; 14 h;
参考文献
Thiebes, Christoph; Prakash, G. K. Surya; Petasis, Nicos A.; Olah, George A.
Synlett, 1998 , # 2 p. 141 - 142
反应条件
iodine cloride in tetrachloromethane 24 h; Heating;
参考文献
Bennetau, Bernard; Rajarison, Florent; Dunogues, Jacques; Babin, Pierre
Tetrahedron, 1993 , vol. 49, # 47 p. 10843 - 10854
反应条件
1: acetic acid; tin (II)-chloride; hydrogen chloride 2: Diazotization View Scheme
参考文献
Scientific Papers of the Institute of Physical and Chemical Research (Japan), , vol. 35, p. 365,369
Chem. Zentralbl., , vol. 110, # I p. 4188
反应条件
K2S; iodine in diethyl ether 24 h; Ambient temperature;
参考文献
Wada, Masanori; Wakamori, Hiroyuki; Hiraiwa, Akira; Erabi, Tatsuo
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1389 - 1391
反应条件
1: toluene; KHCO3 / 100 °C 2: platinum; ethanol / Hydrogenation 3: Diazotization View Scheme
参考文献
Journal of the American Chemical Society, , vol. 55, p. 4225,4227
反应条件
1: With iodine T=20°C; 5 h; 2: With water 0.25 h; Further stages.;
参考文献
Yadav; Kondaji; Shiva Ram Reddy; Srihari
Tetrahedron Letters, 2008 , vol. 49, # 23 p. 3810 - 3813
反应条件
Diazotization.Kochen der Diazoniumsulfatloesung mit KI;
参考文献
Chemische Berichte, , vol. 40, p. 4006
反应条件
in dichloromethane-d2 T=20°C;
参考文献
European Journal of Organic Chemistry, , # 31 p. 7128 - 7138
