1: [1-(2-bromophenyl)ethoxy]diphenyl(trimethylsilyl)silane With azobisisobutyronitrile; tri-n-butyl-tin hydride in benzene
Rearrangement; 7.5 h;
2: methyllithium in benzene
T=20°C; Ring cleavage; desilylation; 12 h; Further stages. Title compound not separated from byproducts.;
1: ([1-(2-bromophenyl)ethoxy]diphenylsilyl)trimethylgermane With azobisisobutyronitrile; tri-n-butyl-tin hydride in benzene
Rearrangement; 7.5 h;
2: methyllithium in benzene
T=20°C; Ring cleavage; desilylation; 12 h; Further stages. Title compound not separated from byproducts.;