1-[2-硝基-4-(三氟甲基)苯基]哌啶合成路线 (共 5 条)
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; 1 h; Product distribution / selectivity;
参考文献
HAGIWARA, Masatoshi
Patent: EP1712242 A1, 2006 ;
Location in patent: Page/Page column 18; 30 ;
反应条件
in N,N-dimethyl-formamide T=0°C; 0.666667 h; Product distribution / selectivity;
参考文献
HAGIWARA, Masatoshi
Patent: EP1712242 A1, 2006 ;
Location in patent: Page/Page column 18; 31 ;
反应条件
/BRN= 102438/ in benzene T=25°C; Rate constant;
参考文献
Journal of the Chemical Society [Section] B: Physical Organic, , p. 1595 - 1600
反应条件
in acetonitrile T=25°C; Kinetics; Further Variations:amine concentration;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1378 - 1383
反应条件
1: With hydrogenchloride; tin(ll) chloride in methanol T=0 - 20°C; 17.5 h; 2: With water; sodium hydrogencarbonate in methanol Product distribution / selectivity;
参考文献
HAGIWARA, Masatoshi
Patent: EP1712242 A1, 2006 ;
Location in patent: Page/Page column 18; 30 ;