(OC-6-11)-六氟-铌酸钾 (1:1)合成路线 （共 4 条）
反应条件
HNO3 in hydrogen fluoride aq. HF; dissoving of NB in 60-percent aq. HF, addition of HNO3, precipitating with solution of KH2F in 60-percent aq. HF;; washing with aq. HF, recrystallization from aq. HF, drying;;
参考文献
Savchenko, G. S.; Tananaev, I. V.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1946 , vol. 19, p. 1093 - 1106
C. A., 1947 , p. 4733
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Gmelin Handbook: Nb: MVol.B4, 9.3.1, page 201 - 202
反应条件
solvent: BrF3; in further solvent(s)
参考文献
Gutmann, V.; Emeleus, H. J.
Journal of the Chemical Society, 1950 , p. 1046 - 1050
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Gmelin Handbook: Nb: MVol.B4, 9.3.1, page 201 - 202
反应条件
in hydrogen fluoride aq. HF; evaporation of solution in a stream of dry N2;; crystallization on cooling down to 0°C;;
参考文献
Xu, Fei; Matsumoto, Kazuhiko; Hagiwara, Rika
Dalton Transactions, 2012 , vol. 41, # 12 p. 3494 - 3502
反应条件
in neat (no solvent) reaction of Nb-powder and KCl with excess BrF3;;
参考文献
Gutmann, V.; Emeleus, H. J.
Journal of the Chemical Society, 1950 , p. 1046 - 1050
Full Text View citing articles Show Details
Gmelin Handbook: Nb: MVol.B4, 9.3.1, page 201 - 202
