反应条件
1: (E)-indanone O-4-trifluoromethylbenzyl oxime With sodium tetrahydroborate; borane; enantiopure spiroborate ester in 1,4-dioxane
36 h;
2: acetic anhydride With 4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0°C; 3 h; Further stages. Title compound not separated from byproducts.;
参考文献
Huang, Xiaogen; Ortiz-Marciales, Margarita; Huang, Kun; Stepanenko, Viatcheslav; Merced, Francisco G.; Ayala, Angel M.; Correa, Wildeliz; De Jesus, Melvin
Organic Letters, 2007 , vol. 9, # 9 p. 1793 - 1795