反应条件
n-butyllithium; magnesium bromide; bis(1,3-diphenylphosphinopropane) nickel(II) chloride 1.) hexane, diethyl ether, r.t., 5 min, reflux, 1 h, 2.) hexane, diethyl ether, 0 deg C, r.t., 0.5 h, 3.) hexane, diethyl ether, 15 h, r.t.; Yield given. Multistep reaction;
参考文献
Eachern, Anita Mac; Soucy, Chantal; Leitch, Leonard C.; Arnason, John T.; Morand, Peter
Tetrahedron, 1988 , vol. 44, # 9 p. 2403 - 2412