4,6-二甲基-2-碘嘧啶合成路线 （共 5 条）
反应条件
hydrogen iodide T=20°C; 5 h;
参考文献
Vlad, Gabor; Horvath, Istvan T.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6550 - 6552
反应条件
1: 75 percent / conc. HCl / ethanol / 24 h / Heating 2: 77 percent / phosphorus oxychloride / 10 h / Heating 3: 62 percent / conc. HI / 5 h / 20 °C View Scheme
参考文献
Vlad, Gabor; Horvath, Istvan T.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6550 - 6552
反应条件
1: 77 percent / phosphorus oxychloride / 10 h / Heating 2: 62 percent / conc. HI / 5 h / 20 °C View Scheme
参考文献
Vlad, Gabor; Horvath, Istvan T.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6550 - 6552
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc 1.) THF, r.t., 6 h, 2.) THF, r.t., 41 h; Yield given. Multistep reaction;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Murata, Naoko; Yamanaka, Hiroshi
Tetrahedron, 1993 , vol. 49, # 43 p. 9713 - 9720
反应条件
2: potassium carbonate; methanol
View Scheme
参考文献
Li, Bo; Wang, Wei-Kang; Zang, Shuang-Quan; Mak, Thomas C.W.
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 173 - 176
