反应条件
in tetrahydrofuran argon atmosphere; addn. of borane-THF complex to soln. of Ph2PCl (-0°C), portionwise addn. of LiAlH4, stirring (0°C, 2 h); pptn. on addn. to aq. HCl (stirring, ice), extn. (benzene), drying of extract (Na2SO4), concn. (vac.), chromy. (silica gel, benzene); elem. anal.;
参考文献
Imamoto, Tsuneo; Oshiki, Toshiyuki; Onozawa, Takashi; Kusumoto, Tetsuo; Sato, Kazuhiko
Journal of the American Chemical Society, 1990 , vol. 112, # 13 p. 5244 - 5252