3,4-二苯基异苯并吡喃-1-酮合成路线 （共 25 条）
反应条件
copper diacetate; air; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in N,N-dimethyl-formamide
T=120°C; 2 h;
参考文献
Ueura, Kenji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2007 , vol. 9, # 7 p. 1407 - 1409
反应条件
[Ni0(1,5-cyclooctadiene)2]; zinc(II) chloride; trimethylphosphane in acetonitrile
T=80°C; 12 h; Inert atmosphere;
参考文献
Kajita, Yuichi; Kurahashi, Takuya; Matsubara, Seijiro
Journal of the American Chemical Society, 2008 , vol. 130, # 51 p. 17226 - 17227
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide
T=85°C; Suzuki reaction;
参考文献
Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5936 - 5942
反应条件
C70H44Cl2F64N2O6Pd2; tetrabutylammomium bromide; sodium carbonate in water
T=150°C; 0.45 h; Microwave irradiationGreen chemistry; Reagent/catalyst; regioselective reaction;
参考文献
Ang, Wei Jie; Tai, Chih-Hsuan; Lo, Lee-Chiang; Lam, Yulin
RSC Advances, 2014 , vol. 4, # 10 p. 4921 - 4929
反应条件
sodium acetate in acetic acid
anodic oxidation;
参考文献
Delaunay, Jacques; Simonet, Jacques
Tetrahedron Letters, 1988 , vol. 29, # 5 p. 543 - 544
反应条件
copper diacetate; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Ueura, Kenji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5362 - 5367
反应条件
1: 93 percent / I2 / CH2Cl2 / 1 h / 20 °C
2: 58 percent / LiCl / Pd(OAc)2 / dimethylformamide / 20 h / 85 °C
View Scheme
参考文献
Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5936 - 5942
反应条件
1: 100 percent / ICl / CH2Cl2 / 0.5 h / 20 °C
2: 58 percent / LiCl / Pd(OAc)2 / dimethylformamide / 20 h / 85 °C
View Scheme
参考文献
Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5936 - 5942
反应条件
1: 99 percent / Et3N / PdCl2(PPh3)2; CuI / 55 °C
2: 93 percent / I2 / CH2Cl2 / 1 h / 20 °C
3: 58 percent / LiCl / Pd(OAc)2 / dimethylformamide / 20 h / 85 °C
View Scheme
参考文献
Yao, Tuanli; Larock, Richard C.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 5936 - 5942
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver(I) acetate; silver carbonate in tert-butyl alcohol
T=120°C; 16 h;
参考文献
Park, Youngchul; Seo, Jungmin; Park, Sangjune; Yoo, Eun Jeong; Lee, Phil Ho
Chemistry - A European Journal, 2013 , vol. 19, # 48 p. 16461 - 16468
