(1α,3α,5α)-1,3,5-环己三腈合成路线 （共 4 条）
反应条件
thionyl chloride in N,N-dimethyl-formamide T=45°C; 15 h;
参考文献
Mayer, Hermann A.; Stoessel, Philipp; Fawzi, Riad; Steimann, Manfred
Chemische Berichte, 1995 , vol. 128, # 7 p. 719 - 724
反应条件
1: 100 percent / SOCl2 / 12 h / Heating 2: 90 percent / pyridine / CH2Cl2 / 12 h / 40 °C 3: 85 percent / liquid NH3 / 15 h / -40 - 20 °C 4: 65 percent / SOCl2 / dimethylformamide / 15 h / 45 °C View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 2 p. 193 - 200
反应条件
1: 90 percent / pyridine / CH2Cl2 / 12 h / 40 °C 2: 85 percent / liquid NH3 / 15 h / -40 - 20 °C 3: 65 percent / SOCl2 / dimethylformamide / 15 h / 45 °C View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 2 p. 193 - 200
反应条件
1: 85 percent / liquid NH3 / 15 h / -40 - 20 °C 2: 65 percent / SOCl2 / dimethylformamide / 15 h / 45 °C View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 2 p. 193 - 200
