三甲基-(三甲基锡烷基甲基)锡烷合成路线 （共 34 条）
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Matsuoka, Hiroharu; Igarashi, Tsutomu; Minomura, Masafumi; Murayama, Eigoro
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1207 - 1212
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 10 min, 2.) -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Sato, Tadashi; Matsuoka, Hiroharu; Igarashi, Tsutomu; Minomura, Masafumi; Murayama, Eigoro
Journal of Organic Chemistry, 1988 , vol. 53, # 6 p. 1207 - 1212
反应条件
iodine in chlorobenzene (N2); monitored by (1)H NMR;
参考文献
Organometallics, , vol. 4, p. 821 - 825
反应条件
bromine in dichloromethane (N2); monitored by (1)H NMR;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
反应条件
Br2 in methanol; tetrachloromethane treatment with Br2 in MeOH/CCl4 at -60°C, warmed;
参考文献
Karol, Thomas J.; Hutchinson, John P.; Hyde, Jeffrey R.; Kuivila, Henry G.; Zubieta, Jon A.
Organometallics, 1983 , vol. 2, p. 106 - 114
反应条件
in tetrachloromethane under N2 at 0°C; not isolated, detected by NMR;
参考文献
Kuivila, Henry G.; Karol, Thomas J.; Swami, Kamal
Organometallics, 1983 , vol. 2, p. 909 - 914
反应条件
in neat (no solvent) heated at 60°C for 12 h; distd. (12-15 Torr), recrystd. (C6H6); elem. anal.;
参考文献
Organometallics, , vol. 2, p. 106 - 114
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; methylene double anion donors, var. esters; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 53, # 6 p. 1207 - 1212
反应条件
acetic acid in acetic acid Kinetics; (N2); monitored by (1)H NMR;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
反应条件
in tetrachloromethane (N2); monitored by (1)H NMR;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
