2-氯-1-甲酰基-1-环己烯合成路线 （共 23 条）
反应条件
1: With trichlorophosphate T=0 - 20°C; 0.5 h; 2: With sodium hydrogencarbonate in water Cooling with ice;
参考文献
Journal of Organometallic Chemistry, , vol. 696, # 1 p. 179 - 187
反应条件
trichlorophosphate anschl. mit Cyclohexanon und H2O;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 24, p. 2385,2390
Org. Synth. Coll. Vol., , vol. V, p. 215
反应条件
trichlorophosphate 1.) CH2Cl2, 0-10 deg C, 30 min; 2.) room temp., 15 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 6 p. 575 - 577
参考文献
Chemistry - A European Journal, , vol. 13, # 14 p. 4074 - 4080
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Sadekov; Nivorozhkin; Zakharov; Minkin
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1387 - 1389
反应条件
1: With pyridine; triethylamine T=10 - 15°C; 1 h; 2: With potassium hydroxide 0.25 h; Cooling with ice;
参考文献
Mavrova, Anelia Ts.; Wesselinova, Diana; Tsenov, Yordan A.; Denkova, Pavletta
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 1 p. 63 - 69
反应条件
1: 63 percent / H2, triethylamine / Palladium/charcoal/KOH / ethanol / 0.75 h 2: 33 percent / acetic acid / 17 h / Heating View Scheme
参考文献
Gangjee; Ohemeng; Lin; Katoh
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 523 - 528
反应条件
in acetic acid 4 h; Heating;
参考文献
Gangjee; Ohemeng; Lin; Katoh
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 523 - 528
反应条件
hydrogen; triethylamine; potassium hydroxide; palladium on activated charcoal in ethanol 0.75 h;
参考文献
Gangjee; Ohemeng; Lin; Katoh
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 2 p. 523 - 528
反应条件
1: diethyl (mercaptomethyl)phosphonate With sodium hydride in tetrahydrofuran T=0°C; 0.25 h; 2: (2-chlorocyclohex-1-enyl)carboxaldehyde in tetrahydrofuran T=20°C; 19 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 55, # 7 p. 1332 - 1335
