4-苯基-1,2,3-三氮唑合成路线 （共 74 条）
反应条件
sodium azide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane T=90°C; 14 h;
参考文献
Barluenga, Jose; Valdes, Carlos; Beltran, Gustavo; Escribano, Maria; Aznar, Fernando
Angewandte Chemie - International Edition, 2006 , vol. 45, # 41 p. 6893 - 6896
反应条件
1: With oxygen; sodium hydrogencarbonate in N,N-dimethyl-formamide T=110°C; 0.0833333 h; 2: With sodium dithionite in N,N-dimethyl-formamide T=110°C; 0.0833333 h; 3: With water in N,N-dimethyl-formamide T=110°C; SolventReagent/catalystTemperature;
参考文献
He, Yun; Sun, Erxiao; Zhao, Yi; Hai, Li; Wu, Yong
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 111 - 115
反应条件
1,1-dimethylethylmagnesium chloride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran; toluene T=20°C; 0.0833333 h;
参考文献
Kamijo, Shin; Huo, Zhibao; Jin, Tienan; Kanazawa, Chikashi; Yamamoto, Yoshinori
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6389 - 6397
反应条件
copper(l) iodide; trimethylsilylazide in methanol; N,N-dimethyl-formamide T=100°C; 11 h;
参考文献
Jin, Tienan; Kamijo, Shin; Yamamoto, Yoshinori
European Journal of Organic Chemistry, 2004 , # 18 p. 3789 - 3791
反应条件
1,1-dimethylethylmagnesium chloride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran; toluene T=20°C; 0.0833333 h;
参考文献
Kamijo, Shin; Huo, Zhibao; Jin, Tienan; Kanazawa, Chikashi; Yamamoto, Yoshinori
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6389 - 6397
反应条件
methanol; magnesium T=25°C; 2 h;
参考文献
Yoo, Eun Jeong; Ahlquist, Marten; Kim, Seok Hwan; Bae, Imhyuck; Fokin, Valery V.; Sharpless, K. Barry; Chang, Sukbok
Angewandte Chemie - International Edition, 2007 , vol. 46, # 10 p. 1730 - 1733
反应条件
potassium tert-butylate in tetrahydrofuran T=-78 - 0°C;
参考文献
Yap, Amy H.; Weinreb, Steven M.
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3035 - 3038
反应条件
sodium azide in dimethyl sulfoxide T=80 - 90°C;
参考文献
Quiclet-Sire, Beatrice; Zard, Samir Z.
Synthesis, 2005 , # 19 art. no. C09005SS, p. 3319 - 3326
反应条件
copper(l) iodide; sodium azide; caesium carbonate; sodium L-ascorbate in dimethyl sulfoxide T=110°C; 4 h; Inert atmosphereSealed tube;
参考文献
Jiang, Yubo; Kuang, Chunxiang; Yang, Qing
Synthesis, 2010 , # 24 art. no. F15610SS, p. 4256 - 4260
反应条件
copper(l) iodide; sodium azide; potassium carbonate; sodium L-ascorbate in dimethyl sulfoxide T=120°C; 12 h; Inert atmosphere;
参考文献
Wang, Xiaokun; Kuang, Chunxiang; Yang, Qing
European Journal of Organic Chemistry, 2012 , # 2 p. 424 - 428
