2,3-二甲基-1-己烯合成路线 （共 11 条）
反应条件
aluminum oxide T=375 - 400°C;
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Full Text Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
反应条件
Ta-η5-C5Me5-(cyclooctene)Cl2 in pentane T=50°C; P=2068.6 Torr; 28 h; Rate constantProduct distributionMechanism;
参考文献
Mclain,S.J.; Sancho,J.; Schrock,R.R.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5610
反应条件
mixed oxide catalyst (26 wt.percent Ce; 47 wt.percent Zr; 1.54 wt.percent S) calcined to 700 C in flowing air for 3 h T=200 - 220°C; P=3345.86 Torr; 23 - 65 h; Gas phase; Product distribution / selectivity;
参考文献
EXXONMOBIL CHEMICAL PATENTS INC.
Patent: WO2005/66101 A1, 2005 ;
Location in patent: Page/Page column 25 ;
反应条件
1: 1,2-hexandiene With lithium in pentane T=40°C; 12 h; 2: dimethyl sulfate in pentane Further byproducts given;
参考文献
Maercker, Adalbert; Tatai, Andrea; Grebe, Burkhard; Girreser, Ulrich
Journal of Organometallic Chemistry, 2002 , vol. 642, # 1-2 p. 1 - 8
反应条件
T=350 - 400°C; Produkt 5: 2.3-Dimethyl-hexen-(3);
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Full Text Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
反应条件
T=250°C; Produkt 5: 2.3-Dimethyl-hexen-(3);
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Full Text Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
反应条件
1: Alkaline hydrolysis View Scheme
参考文献
Maercker, Adalbert; Tatai, Andrea; Grebe, Burkhard; Girreser, Ulrich
Journal of Organometallic Chemistry, 2002 , vol. 642, # 1-2 p. 1 - 8
反应条件
1: Alkaline hydrolysis View Scheme
参考文献
Maercker, Adalbert; Tatai, Andrea; Grebe, Burkhard; Girreser, Ulrich
Journal of Organometallic Chemistry, 2002 , vol. 642, # 1-2 p. 1 - 8
参考文献
Maercker, Adalbert; Tatai, Andrea; Grebe, Burkhard; Girreser, Ulrich
Journal of Organometallic Chemistry, 2002 , vol. 642, # 1-2 p. 1 - 8
反应条件
Produkt 5: 2.3-Dimethyl-hexen-(3);
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Full Text Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
